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By employment of sulfonate-decorated metal–organic cuboctahedra (MOCs) as tectons, we report an interesting example of molecular tectonics strategy for the rational construction of three-dimensional (3D) porous network 1 through complementary and metrically matched N–H+···–O–S hydrogen bonds between guanidinium and sulfonate (GS) moieties. Built from the MOCs as 24-connected nodes ...
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